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Beilstein J. Org. Chem. 2011, 7, 386–393, doi:10.3762/bjoc.7.49
Graphical Abstract
Figure 1: Methods for synthesis of dibromides I and their use for preparation of 6-membered heterocycles.
Scheme 1: General methods for preparation of diols VII.
Scheme 2: General methods for preparation of tetrahydropyrans VIII.
Figure 2: Structures of 1,5-dibromomopentanes 1a–1d.
Scheme 3: Preparation of dibromides 1.
Scheme 4: Preparation of diol 2a.
Scheme 5: Preparation of diol 2b.
Scheme 6: Preparation of tetrahydropyrans 3a–3c.
Scheme 7: Preparation of tetrahydropyran 3d.
Scheme 8: Preparation of methylenetetrahydropyrans 6.
Scheme 9: Preparation of bromides 8 and 10.
Scheme 10: Preparation of sulfonium derivatives 11.